Petrowidada’s world-scale plant in East Java, Indonesia. Source: Clariant
Clariant (Muttenz, Switzerland; www.clariant.com) announced the successful startup of its new high-yield OxyMax PA 690 catalyst at Petrowidada’s world-scale phthalic anhydride plant in Gresik, East Java, Indonesia. After an industry-standard ramp-up time to a high ortho-xylene load of 100 grams per normal cubic meter (g/Nm³), the production facility reports significantly greater yield for the first nine months of operation. The highly favorable results demonstrated at the Petrowidada plant are due to the unique design and materials employed in the new catalyst.
OxyMax PA 690 is a shell-type catalyst that is produced using Clariant’s proprietary fluid-bed coating technology. In the process, the catalytically active materials titaniumdioxide and vanadium-pentoxide along with special promoters are coated in a thin shell on ceramic rings. The thin, porous shell resolves mass and heat transport challenges during selective oxidation of ortho-xylene to phthalic anhydride (PA). Hence, over-oxidation is reduced, and unwanted by-products, such as carbon oxides and maleic anhydride, are minimized. The shell, combined with an improved catalyst composition and optimized mass transport properties, results in excellent selectivity and up to 116 wt.% reactor outlet PA yield.
Thanks to its unique composition and formulation developed in a multi-year R&D project, the new OxyMax PA 600 catalyst series has been granted two patent families. The new PA catalyst is the result of instrumental research and development performed by Dr. Gerhard Mestl, Head of Oxidation Catalysts R&D at Clariant, and his team. For his work in applied selective oxidation, Dr. Mestl received the prestigious Applied Catalysis Award from the European Federation of Catalysis Societies (EFCATS) in 2017.
Petrowidada is one of the largest producers of phthalic anhydride in Southeast Asia and the sole producer in Indonesia. The company’s plant in East Java has successfully used previous generations of Clariant’s high-ortho-xylene-load PA catalysts since 2007. With OxyMax PA 690, the facility has experienced an increase in overall plant yield of 1 wt.%, and benefits from excellent PA quality with low impurity levels at the reactor outlet. Considering the plant’s annual capacity of 70,000 metric tons of phthalic anhydride, the superior productivity afforded by the new catalyst translates into considerable benefits for the producer.
Mr. Jaka Lelana, Plant Director at Petrowidada, expressed his satisfaction with the new catalyst, stating, “Given the scale of our phthalic anhydride business, efficiency is key to our continued success. That’s why we are particularly enthusiastic about the performance of the new catalyst, and confident that it will open new avenues for growth.”
Stefan Heuser, Senior Vice President & General Manager Business Unit Catalysts at Clariant, added, “We have successfully supported Petrowidada for more than a decade. It is close partnerships such as this that reveal valuable insights into our customers’ needs and challenges, and ultimately result in true breakthroughs in catalyst development like OxyMax PA 690.”