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Chemical Engineering

This lube-oil analyzer features triple-cell FTIR technology

| By Mary Bailey

This company has expanded the technical capabilities of its eraspec oil technology, a portable, stand-alone Fourier-transform infrared (FTIR) lubricant analyzer. Designed to deliver laboratory-grade precision directly to onsite environments, the lube-oil analyzer utilizes a fully automated, solvent-free workflow with an integrated sample pump. To address increasingly demanding field requirements, the analyzer is equipped with three advanced hardware and software features designed to enhance trace-level detection, water quantification and rapid product verification: triple-cell design, chemometric water quantification and automated fingerprinting.

eralytics lube oil analyzer

Source: eralytics

The hardware integrates an additional 500-µm measurement cell alongside the standard 100-µm cell and a built-in reference cell. This dual-path-length configuration improves the Limit of Detection (LOD) for antioxidant additives (such as phenolic antioxidants), water and esters. The analyzer’s software automatically calculates and reports the result using the 500-µm cell when concentrations fall below a standard threshold.

Eraspec oil also provides a chemometric model for the determination of water, calibrated to ASTM D6304-B (Karl Fischer oven method). The model utilizes specific spectral regions to isolate water absorption, while avoiding interferences from oxidation products and oil additives. For water concentrations of 50 ppm or higher, this doubles analytical performance compared to direct FTIR methods, while still providing results in under two minutes.

FTIR spectral matching using the eraspec oil analyzers provides an objective method for product identification of fresh lubricating oils. This capability verifies an unknown lubricant’s unique molecular fingerprint by cross-referencing its spectrum against an on-board reference database. The analytical process relies on a matching algorithm that calculates a Pearson correlation coefficient to determine the optimal product match. This new feature was developed to enhance process reliability and optimize incoming goods inspections. — eralytics GmbH, Vienna, Austria

www.eralytics.com