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A single flow reactor produces a toxic precursor, an unstable reagent and product

The Vilsmeier reagent (VR), [(CH3)2 NCHCl]Cl, is necessary for producing a large range of pharmaceuticals, but it is unstable in air and is made from the toxic precursor phosgene (COCl2). A new flow-reactor system has been developed by Akihiko Tsuda,…

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First-phase pilot tests completed to demonstrate RotoDynamic technology

Coolbrook Oy (Helsinki, Finland; www.coolbrook.com) has successfully completed the first phase of large-scale pilot testing (photo) for its RotoDynamic Technology at the Brightlands Chemelot Campus in Geleen, the Netherlands. During 2023, Coolbrook has been running a test program to demonstrate…

Chementator Briefs

Bio-acrylonitrile Site selection is underway for a glycerol-to-acrylonitrile demonstration-scale plant that will enable the production of plant-based acrylonitrile (ACN). Trillium (Knoxville, Tenn.; www.trilliumchemicals.com) is partnering with Zeton (Oakville, Ont.; www.zeton.com) to design and build the plant, known as Project Falcon.…

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Closed-loop CO2-based energy-storage system slated for Wisconsin

Alliant Energy (Madison, Wis.; www.alliantenergy.com) was recently selected to receive a $30-million grant from the U.S. Dept. of Energy’s Office of Clean Energy Demonstrations (OCED; Washington, D.C.; www.energy.gov/oced) for a proposed 200-MWh energy storage system. Alliant Energy’s new battery system,…

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A new heat-resistant membrane

Most polymeric membranes degrade during use, making them impractical for industrial separation processes. To solve this problem, researchers from the State University of New York at Buffalo (SUNY Buffalo; www.buffalo.com), with cooperation for scientists at Rensselar Polytechnic Institute, have created…

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Ultrathin films achieve record hydrogen separation

Scientists at École Polytechnique Fédérale de Lausanne (EPFL; Switzerland; www.epfl.ch) have synthesized the first ever metal-organic frameworks (MOFs) membrane with the thickness of just one unit cell. The ultrathin film yields record-high performance for the separation of hydrogen from nitrogen.…

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Commercial Progress on Turquoise Hydrogen

Producing hydrogen via methane pyrolysis – termed ‘turquoise hydrogen’ – has thus far received less attention than ‘blue’ and ‘green’ H2, but it may offer advantages over both While the vast majority of current hydrogen production occurs by steam reforming…

Facts At Your Fingertips: Wet and Dry Milling

Milling is a common technique for controlling particle-size distribution (PSD) in solid products through size reduction and surface modification. Broadly, mills can be categorized as wet or dry mills, and these two categories are each further subdivided by how comminution…

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Modular Construction Encourages New Applications

The efficiency and cost effectiveness of modularity provides advantages for small- and large-scale projects When the right conditions exist, the benefits of modular construction — from laboratory scale to large scale — are plentiful and allow single-source, cost-effective and efficient…

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Business News: November 2023

Plant Watch BASF to build a new fermentation plant in Ludwigshafen October 12, 2023 — BASF SE (Ludwigshafen, Germany; www.basf.com) is investing in a new fermentation plant for biological crop-protection products, such as fungicides, insecticides and seed treatments, at its…