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Tower Doctor: Can Trash Interfere With a Cure?

Henry Kister shares lessons learned from troubleshooting distillation towers Construction of new production units has an undesirable byproduct: trash. Sometimes the hard question is­— Who will clean? The author was the startup superintendent on a new unit in an olefins…

Facts at your Fingertips: Clean-in-Place (CIP) Systems

Cleaning equipment surfaces is critical for processes involving biological materials to prevent microbial contamination. Clean-in-place (CIP) systems play a key role. In addition to preventing contamination, CIP systems also remove grit, scale and organic matter, which may affect process performance.…

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Tower Doctor: Should the Doctor Believe a Flowmeter?

Henry Kister shares lessons learned from troubleshooting distillation towers Many cooling-water systems do not have flowmeters. This is a tale about a cooling-water flowmeter that made a difference. As a startup superintendent at ICI Australia in the late 1970s, the…

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A Primer on pH Measurement

Understanding the basic principles of operation and construction designs of glass membrane sensors can help in choosing the right pH sensor One of the most critical measurements in liquid chemical processing is pH. In this article, the importance of the…

Detecting and Preventing Spills and Leaks

Comprehensive planning, along with appropriate level-measurement technologies and safety instrumented systems, can empower plant personnel to significantly reduce the likelihood and severity of hazardous chemical spills In most industries that manufacture, use or store chemicals and other hazardous liquids, a…

Facts At Your Fingertips: Physical Gas-Separation Methods

Industrial gases are critical for a wide range of applications throughout the chemical process industries (CPI). Many of these gases must be separated from others, such as nitrogen from air, or hydrogen from natural gas using physical gas-separation techniques that…

Technology Profile: Production of EPDM Rubber

Ethylene propylene diene monomer (EPDM) rubber is a terpolymer elastomer derived from ethylene and propylene, along with small amounts of a non-conjugated diene as a third monomer (Figure 1). With a completely saturated polymer backbone, this random elastomeric copolymer exhibits…

Gas Trapping Can Unsettle Distillation Columns

Operational troubleshooting guidance is provided for several scenarios involving trapped non-condensable gases in distillation towers Non-condensable gases are often present in distillation towers, either expectedly or unexpectedly. When they do appear, or when the quantity of non-condensable gases varies from…

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Facts At Your Fingertips: Predictive Maintenance Methods

Predictive maintenance (PdM) programs can provide advanced warning of equipment problems and potential failures. This one-page reference provides brief descriptions of six common predictive maintenance methods. Infrared thermography Continuous monitoring of equipment temperature over time has the potential to identify…

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Technology Profile: Production of L-Lysine

Lysine (Figure 1) is an α-amino acid used in the biosynthesis of proteins. The compound contains an amino group and a carboxylic acid group. Under biological conditions, the amino group is protonated (–NH3+) and the carboxylic acid group is deprotonated…