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How to Prepare a Process Design Basis

    Intelligent — and thorough — preparation of a process-design-basis document can make the difference between a high-quality design for a chemical-process project and a poor one. The process-design-basis document represents the owner’s instructions to the design engineering organization…

Infrared Temperature Monitoring: Know the Right Questions to Ask

The infrared approach to temperature monitoring is especially useful in situations where process temperatures are extremely high, the target is in motion, and the need to avoid contaminants is significant Accurate temperature measurement can often be quite challenging, especially in…

Predicting Powder Flow Behavior – A New Approach

When faced with the complexity of predicting powder flow, it is tempting to reduce a material’s flow behavior to a single number or even a flow function. The method presented here, however, compiles a number of relevant parameters into a…

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Don’t Overlook Composite FRP Pipe

    There are several reasons why composite fiberglass-reinforced-plastic (FRP) pipe has been replacing conventional pipe, and why this still relatively new material (see box, p. 46) should be kept in mind whenever piping is being specified for a new…

Preventing Fires and Explosions in Pilot Plants

    Among pilot plants, those in petrochemical or petroleum-refining service pose special risks of fire and/or explosion. The key strategies to minimize those risks are these: properly conducted preconstruction safety reviews; leaktight design and construction; close attention to area…

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A Bit of Extra Lab Effort Can Prevent Grief During Scaleup

    It’s an old saw, but I’ve long held that process development is very much a team effort. Developing safe, robust and scaleable chemical processes calls for close collaboration between synthesis chemists, process development engineers and pilot plant personnel.…

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Will Mass Flow Solve All Your Segregation Problems?

Most chemical processes must produce products that are uniformly mixed. There have been many articles written about preventing particle segregation during bulk solids flow; and ensuring a mass flow pattern is a common suggestion. But mass flow alone is not…

Understanding Atmospheric Storage Tanks

    Liquids are accumulated and stored in tanks of various shapes and sizes throughout the chemical process industries (CPI). A small number of companies have made the design, fabrication and erection of these vessels their specialty. Initially, however, it…

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Mixing Systems: Design and Scale Up

    Fundamental to the chemical process industries (CPI) — whether specialty or bulk chemicals, pharmaceuticals, food products, minerals processing, environmental protection or other products or activities — is the need for mixing. The wide variety and complexity of mixing…

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Distillation: How to Specify & Install Cartridge Trays

Cartridge trays, defined below, can be the perfect hardware solution for distillation columns that are less than 3 feet (0.9m) in diameter and have a unique need for trays. Packing is usually the preferred choice for small-diameter columns, but there…